2024 – Evaluating innovative materials based on multi-element tungsten alloys and advanced manufacturing processes

Evaluating innovative materials based on multi-element tungsten alloys and advanced manufacturing processes

2024 Research Campaign, Thrust: FPP Candidate Wall Materials

Purpose of Experiment

This experiment aims to comprehensively evaluate the performance of advanced tungsten-based materials under the extreme conditions of a tokamak divertor. Tungsten, a primary candidate for plasma-facing components due to its high melting point, low sputtering yield, and good thermal conductivity, suffers from brittleness and embrittlement under neutron damage. This study will test several innovative tungsten materials, including Dispersoid-Strengthened Tungsten (DSW), tungsten-based multiple principle element alloys (MPEAs), tungsten heavy alloys (WHA), and various tungsten composites and coatings. The objective is to improve the materials’ resistance to erosion, cracking, and hydrogen retention, thereby enhancing their suitability for future fusion reactors.

Experimental Approach

The experiment will utilize the Divertor Material Exposure Station (DiMES) in the DIII-D tokamak to expose small samples of advanced tungsten materials exclusively to ELMy H-mode plasmas.
The materials to be tested include:
1. Dispersoid-Strengthened Tungsten (DSW) with transition metal carbides (e.g., TaC, TiC, ZrC).
2. Tungsten-based Multiple Principle Element Alloys (MPEAs) such as W-Mo-Nb-Ta, W-Cr-V, and W-Ta-Ti.
3. Tungsten Heavy Alloys (WHA) containing Ni, Cu, or Fe.
4. Tungsten composites reinforced with SiC fibers (Wf/W, SiC/W, and SiC-W/W).
5. Plasma-sprayed tungsten coatings (PS-W).
The DiMES probe will be used to expose these materials to high heat and particle fluxes to simulate the conditions of a fusion reactor divertor. The experimental setup will involve multiple DiMES heads with flush and angled samples, subjected to high-power H-mode discharges with ELMy conditions to maximize the assessment of erosion, thermal resilience, and surface morphology changes.
Key aspects of the experimental approach include:
● DSW Samples: Various compositions with optimized microstructures and pre-implanted with helium to investigate the impact of thermal shock events, recrystallization, and erosion under H-mode conditions.
● MPEA Samples: Investigation of preferential sputtering, erosion rates, and hydrogen retention to determine the effects of alloy composition on material performance.
● WHA Samples: Evaluation of the ductility and thermal fatigue resistance under high heat flux conditions.
● Tungsten Composites: Testing of crack propagation, pseudo-ductility, and thermal performance of SiC fiber-reinforced tungsten composites.
● Plasma-Sprayed Coatings: Assessment of the resilience and performance of in-situ plasma-sprayed tungsten coatings under high heat flux conditions.
Post-exposure analyses will include scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS), thermal desorption spectroscopy (TDS), and various spectroscopic techniques to evaluate surface damage, composition changes, and deuterium retention. The results will inform the optimization of tungsten-based materials for improved performance in the extreme environment of a fusion reactor. By integrating these diverse approaches, this experiment aims to provide a comprehensive understanding of the performance and optimization potential of advanced tungsten-based materials for future fusion reactors.

Interested in a behind-the-scenes look at DIII-D? Join us for a virtual OR in-person tour during Fusion Energy Week (May 5-9)! Sign up for a tour here.

X